1.1 This practice covers procedures for the extraction of volatile and semi-volatile organic compounds from water and its headspace using solid-phase microextraction (SPME).<\/p>\n
1.2 The compounds of interest must have a greater affinity for the SPME-absorbent polymer or adsorbent or combinations of these than the water or headspace phase in which they reside.<\/p>\n
1.3 Not all of the analytes that can be determined by SPME are addressed in this practice. The applicability of the absorbent polymer, adsorbent, or combination thereof, to extract the compound(s) of interest must be demonstrated before use.<\/p>\n
1.4 This practice provides sample extracts suitable for quantitative or qualitative analysis by gas chromatography (GC) or gas chromatography-mass spectrometry (GC-MS).<\/p>\n
1.5 Where used, it is the responsibility of the user to validate the application of SPME to the analysis of interest.<\/p>\n
1.6 The values stated in SI units are to be regarded as the standard.<\/p>\n
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section .<\/p>\n
| PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
|---|---|---|---|---|---|---|---|
| 1<\/td>\n | Scope Referenced Documents Terminology Summary of Practice Significance and Use <\/td>\n<\/tr>\n | ||||||
| 2<\/td>\n | Principles of SPME Interferences The Technique of SPME FIG. 1 <\/td>\n<\/tr>\n | ||||||
| 3<\/td>\n | Selection of Fiber Phase Apparatus Reagents Hazards FIG. 2 FIG. 3 <\/td>\n<\/tr>\n | ||||||
| 4<\/td>\n | Sample Handling Optimizing SPME Sampling Parameters Quality Control TABLE 1 <\/td>\n<\/tr>\n | ||||||
| 5<\/td>\n | Procedure Calibration, Standardization and Analysis Precision and Bias Keywords <\/td>\n<\/tr>\n | ||||||
| 6<\/td>\n | REFERENCES <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" D6520-06 Standard Practice for the Solid Phase Micro Extraction (SPME) of Water and its Headspace for the Analysis of Volatile and Semi-Volatile Organic Compounds<\/b><\/p>\n |