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BSI PD IEC/TS 62607-4-6:2018

$102.76

Nanomanufacturing. Key control characteristics – Nano-enabled electrical energy storage. Determination of carbon content for nano-enabled electrode materials, infrared absorption method

Published By Publication Date Number of Pages
BSI 2018 18
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IEC TS 62607-4-6:2018(E) provides a method for determination of carbon content of nano electrode materials by infrared absorption spectroscopy method. The method is applicable to carbon contents of mass fraction between 0,001 % and 100 %. This method will enable customers to: a) decide whether or not a nano electrode material is usable, and b) select a nano electrode material with suitable carbon content for its application. This document includes:   – recommendations for sample preparation,   – outlines of the experimental procedures used to measure electrode nanomaterial properties,   – methods of interpretation of results and discussion of data analysis, and – case studies.

PDF Catalog

PDF Pages PDF Title
2 undefined
4 CONTENTS
5 FOREWORD
7 INTRODUCTION
8 1 Scope
2 Normative references
3 Terms, definitions and abbreviated terms
3.1 Terms and definitions
9 3.2 Abbreviated terms
4 Reagents and materials
4.1 Analysis gas
4.2 Carrier gas
4.3 Fluxes
4.4 Certified reference materials
5 Apparatus
5.1 Analytical balance
10 5.2 Powder compressor
5.3 High-frequency infrared ray carbon/sulfur analyzer
5.4 Muffle furnace
5.5 Crucibles
6 Test methods
6.1 General
6.2 Sample preparation
6.2.1 Drying
Tables
Table 1 – Recommended working conditions of high frequencyinfrared carbon and sulfur analyzer
11 6.2.2 Tableting
6.3 Start up
6.4 Blank verification and determination
6.5 Checking and calibration
6.6 Analysis
6.7 Reporting the results
12 7 Data verification
8 Test report
13 Annex A (informative) Case study
A.1 The gas path diagram and the light path diagram
Figures
Figure A.1 – The gas and light (dashed box) path diagram
14 A.2 Procedures of sample preparation and carbon content determination
Figure A.2 – A-B-C Procedures of sample preparation and carbon content determination
15 A.3 Data analysis for carbon content determination
Table A.1 – Measurement method consistency and measurement results ofdifferent samples in the same laboratory
16 Table A.2 – Inter-laboratory consistency and measurement results of the same sample
17 Bibliography
BSI PD IEC/TS 62607-4-6:2018
$102.76