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BS ISO 19272:2015

$167.15

Low alloyed steel. Determination of C, Si, Mn, P, S, Cr, Ni, Al, Ti and Cu. Glow discharge optical emission spectrometry (routine method)

Published By Publication Date Number of Pages
BSI 2015 42
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PDF Catalog

PDF Pages PDF Title
6 Foreword
7 1 Scope
2 Normative references
8 3 Principle
4 Apparatus
4.1 Glow discharge optical emission spectrometer
4.1.1 General
4.1.2 Short term stability
4.1.3 Detection limit
4.1.4 Data acquisition and processing system
4.1.5 Others
9 5 Sampling
6 Procedure
6.1 Sample preparation
6.2 Selection of spectral lines
10 6.3 Optimization of the instrument
6.3.1 General
6.3.2 Setting the discharge parameters of a direct current (DC) source
11 6.3.3 Setting the discharge parameters of radiofrequency (RF) source
12 6.3.4 Optimization of the detection system
6.3.5 Pre-burning time and integration time
6.3.6 Validation of the instrumental parameters
6.4 Calibration
13 6.5 Checking of the trueness of the method
6.6 Drift correction
6.7 Analysis of the samples
7 Expression of results
7.1 Method of calculation
7.2 Precision
17 8 Test report
18 Annex A (informative) Detection limit
20 Annex B (informative) Additional information on international interlaboratory test
28 Annex C (informative) Graphical representation of precision data
38 Bibliography
BS ISO 19272:2015
$167.15