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BS ISO 11775:2015

$167.15

Surface chemical analysis. Scanning-probe microscopy. Determination of cantilever normal spring constants

Published By Publication Date Number of Pages
BSI 2015 36
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PDF Catalog

PDF Pages PDF Title
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
10 4 Symbols and abbreviated terms
12 5 General information
5.1 Background information
13 5.2 Methods for the determination of AFM normal spring constant
6 Dimensional methods to determine kz
6.1 General
6.2 kz using formulae requiring 3D geometric information
6.2.1 Method
15 6.2.2 Measuring the required dimensions and material properties of the cantilever
16 6.2.3 Determining kz for the rectangular cantilever
6.2.4 Determining kz for the V-shaped cantilever
17 6.2.5 kz for the trapezoidal cross-sections
6.2.6 kz to account for coatings
18 6.3 kz using plan view dimensions and resonant frequency for rectangular tipless cantilevers
6.3.1 Determining kz 
19 6.3.2 Uncertainty
7 Static experimental methods to determine kz
7.1 General
7.2 Static experimental method with a reference cantilever
7.2.1 Set-up
20 7.2.2 Determining kz
22 7.2.3 Uncertainty
23 7.3 Static experimental method using a nanoindenter
7.3.1 General
7.3.2 Determining kz for a tipped or tipless cantilever
24 7.3.3 Uncertainty
26 7.4 Measurement methods
7.4.1 Static deflection calibration
8 Dynamic experimental methods to determine kz
8.1 General
8.2 Dynamic experimental method using thermal vibrations using AFM
8.2.1 Determining kz 
28 8.2.2 Uncertainty
29 Annex A (informative) Inter-laboratory and intra-laboratory comparison of AFM cantilevers
32 Bibliography
BS ISO 11775:2015
$167.15