{"id":462792,"date":"2024-10-20T10:24:21","date_gmt":"2024-10-20T10:24:21","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-101792024\/"},"modified":"2024-10-26T19:18:00","modified_gmt":"2024-10-26T19:18:00","slug":"bs-en-101792024","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-101792024\/","title":{"rendered":"BS EN 10179:2024"},"content":{"rendered":"
This document specifies a spectrophotometric method for the determination of nitrogen in steels. The method is primarily intended for the determination of total nitrogen in very low contents in non-alloy steels. It can be used, however, for any low nitrogen ferrous alloy that is soluble in hydrochloric acid provided that the acid-resistant form of silicon nitride is not present. These highly resistant nitrides have been found only in samples of silicon steels manufactured without aluminium addition and then only in sheet material. The method is applicable to nitrogen contents from 0,000 5 % (by mass) to 0,005 % (by mass). The precision data of the present method are given in Annex A.<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
5<\/td>\n | European foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 5 Reagents <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 6 Apparatus <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | Figure 1 \u2014 Cation exchange column <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | Figure 2 \u2014 Example of aluminium alloy heating block <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | Figure 3 \u2014 Steam distillation apparatus <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 7 Sampling 8 Procedure 8.1 Test portion 8.2 Blank test 8.3 Preparation of the steam distillation apparatus <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 8.4 Determination 8.4.1 Preparation of the test solution 8.4.2 Distillation 8.4.3 Development of the colour <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 8.4.4 Spectrophotometric measurements 8.5 Establishment of the calibration curve 8.5.1 Preparation of the calibration solutions Table 1 \u2014 Calibration solutions 8.5.2 Spectrophotometric measurements <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 8.5.3 Plotting the calibration curve 9 Expression of results 10 Test report <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | Annex A (informative) Precision data Table A.1 \u2014 Statistical information <\/td>\n<\/tr>\n | ||||||
19<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Steels. Determination of nitrogen (trace amounts). Spectrophotometric method<\/b><\/p>\n |