{"id":338116,"date":"2024-10-19T23:39:12","date_gmt":"2024-10-19T23:39:12","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-168012016\/"},"modified":"2024-10-25T22:45:08","modified_gmt":"2024-10-25T22:45:08","slug":"bs-en-168012016","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-168012016\/","title":{"rendered":"BS EN 16801:2016"},"content":{"rendered":"
This European Standard describes a method for the determination of monomethylmercury (MMHg) in foodstuffs of marine origin. The method has been validated in an interlaboratory test on mussel tissue, squid muscle, crab claw muscle, dog fish liver, whale meat, cod muscle and Greenland halibut muscle (all freeze-dried) with mass fractions from 0,04 mg\/kg to 3,6 mg\/kg dry weight according to ISO 5725-2 [1].<\/p>\n
Laboratory experiences have shown that this method is also applicable on fresh samples [2].<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
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4<\/td>\n | Contents Page <\/td>\n<\/tr>\n | ||||||
5<\/td>\n | European foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | 1 Scope 2 Normative references 3 Principle 4 Reagents 4.1 General <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | 5 Apparatus and equipment <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 6 Procedure 6.1 Calculation of optimal spike amount Table 1 \u2014 Isotopic composition of natural Hg and recommended 201Hg enriched spike <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 6.2 Sample preparation 6.3 ICP-MS conditions Table 2 \u2014 Example of instrument settings for ICP-MS <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 6.4 GC conditions Table 3 \u2014 Example of instrument settings for capillary GC 6.5 Set up procedures for the ICP-MS and GC-ICP-MS 6.6 Sample measurement 6.6.1 Preparation of the GC-ICP-MS for analysis <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 6.6.2 Determination of samples and blank solution 6.6.3 Quality control 7 Calculation <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 8 Precision 8.1 General 8.2 Repeatability <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 8.3 Reproducibility Table 4 \u2014 Mean values, repeatability (r) and reproducibility (R) limits 9 Test report <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | Annex A (informative) Precision data Table A.1 \u2014 Precision data Table A.2 \u2014 Trueness based on NRCC DOLT 4 (Dog fish liver) <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Foodstuffs. Determination of elements and their chemical species. Determination of methylmercury in foodstuffs of marine origin by isotope dilution GC-ICP-MS<\/b><\/p>\n |